Detection of Blood Lead Content by Graphite Furnace Method
نویسندگان
چکیده
منابع مشابه
Micromethod for lead determination in whole blood by atomic absorption, with use of the graphite furnace.
I describe a micro-scale method for determining lead in whole blood by utilizing a graphite furnace. Sample pretreatment consists of fivefold dilution with a dilute surfactant. The method is directly calibrated with lead standards prepared in dilute HNO3. To eliminate a small, nonspecific absorption signal from the blood matrix, simultaneous background correction is used. Interlaboratory co...
متن کاملGraphite furnace atomic absorption spectroscopic measurement of blood lead in matrix-matched standards.
Now that the level of concern for a toxic blood lead concentration is 0.482 mumol/L (10 micrograms/dL), laboratories must meet new requirements to shorten analysis times and increase accuracy and precision of blood lead determinations. We used a matrix-matching method to estimate the lead concentration in blood by graphite furnace atomic absorption spectroscopy (GFAAS). For CDC proficiency samp...
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According to a recent CDC report, blood lead concentrations in 1 000 000 US children are at values associated with irreversible damage to health (1 ). The effects of chronic lead poisoning on the developing nervous systems have been well documented (2 ), with children in inner city neighborhoods, where older housing stocks have deteriorating lead paint, most vulnerable (3 ). Accurate screening ...
متن کاملImproved sample preparation for accurate determination of low concentrations of lead in whole blood by graphite furnace analysis.
The effect of low concentrations of lead on pre- and post-natal growth and development is a current concern. We describe a simple method of sample preparation for direct determination of lead in whole blood by Zeeman graphite-furnace atomic absorption spectrometry. This procedure improves analytical precision and accuracy of lead determinations at low concentrations as compared with published f...
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This method was developed to improve sensitivity and eliminate time consuming, evaporative pre-concentration in AOAC Method 973.82 and American Society for Testing and Materials method C738 for testing foodware. The method was developed using leach solutions obtained by leaching 9 differently decorated ceramic vessels with 4% acetic acid for 24 h at room temperature. Lead and cadmium concentrat...
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ژورنال
عنوان ژورنال: Asian Journal of Chemistry
سال: 2014
ISSN: 0970-7077,0975-427X
DOI: 10.14233/ajchem.2014.15845